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Extensive study of the TEM photos (G) out of graphite needles within the samples expanding immediately after 8 min on the 2nd broadening techniques in the step one,600 W demonstrably displays the fresh stage conversion procedure away from graphite in order to diamond. The new white packets are the section to your involved increased images and you may FFT images lower than, as well as the red-colored and you may white arrows indicate the new flat range. (H) and (H-1) are the HADDF and you will bright profession TEM images for another graphite needle, respectively, on the related expanded pictures and FFT photographs less than. The brand new EELS spectra (I) of one’s some other sites marked from the red-colored points of various other phase converting needle found within the (H)/(H-1).
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(J)/(J-1) Drawing of your phase conversion of graphite to diamond in the graphite needle adult for the cauliflower-for example dirt. Understand it incredible periodicity developing processes, HRTEM measurements on the freshly formed covering were performed (Fig. 2). The brand new 0-s attempt (Fig. 2A) displays higher rod-including diamond deposits evidenced because of the diffraction spots from the diamond (111) orientation in the inset Fourier changes (FFT) picture.
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